Moisture Analyzer DewTector

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DTR-A – Automatic Version for Online Measurement

Measuring Moisture of Bulk Solids

The DewTector from Coperion is a measuring device for determining the moisture content of bulk materials, particularly plastic pellets.

The DewTector Story

THE ISSUE

Customers frequently approach Coperion with concerns about product moisture.
•    Plastic manufacturers often face the issue of moisture entering the final product. There are many causes for this: insufficient drying, defective water separators, leaking wash nozzles, condensation, rain, etc. If this goes unnoticed and the product is delivered, it leads to complaints that are associated with high costs and loss of reputation.
•    Processors must adhere to a maximum moisture content to produce high-quality products.
•    In the recycling sector, contaminants are removed through washing, but dry product is needed in the further process.
Nevertheless, product moisture is often not measured or only sporadically, for example, through manual measurement of relative humidity in bags, big bags, etc. This approach is always labor-intensive, mostly non-standardized, and unreliable in detecting moisture.

THE CHALLENGE

Therefore, Coperion has intensively examined the technologies available on the market for automated moisture measurement in the process. These are still not widely used. Here’s why:

→  Established methods such as capacitive moisture measurement or microwave resonance methods are complex and expensive. These indirect methods measure properties such as the dielectric constant and determine the moisture content indirectly through calibration functions that must be determined carefully beforehand.

→ The problem is also that these properties change not only due to moisture, but also, for example, when the composition of the additives in plastics changes. Therefore, a separate calibration would need to be created for each formulation – an unacceptable expense. If the additive content fluctuates, as is particularly the case with surface-applied additives, reliable measurement becomes impossible.

The result was sobering: There is no simple, reliable, and affordable measuring system available on the market that meets the requirements of the plastics industry.

THE SOLUTION

Coperion has therefore decided to develop its own measuring system – focusing on applicability and reliability. The solution is as simple as it is brilliant: Removing moisture by a flow of pressurize air and water-specific detection using a moisture sensor, along with a sophisticated algorithm for analyzing the drying process and determining the amount of moisture – the birth of the Coperion DewTector!

The DewTector Principle

A continuous partial flow for measurement is supplied to the DewTector via a simple branch from a gravity pipe or a higher container. The bulk solid is introduced into a product chamber, which can be pressure-tight separated from the feed and discharge lines by butterfly valves at both the top and bottom.
During the measurement process, a defined amount of air flows through the product chamber and absorbs moisture from the product, which is thereby dried. Thanks to the patented design of the product chamber, the flow is efficiently guided through the product. The air stream exiting the product chamber is directed to the analysis unit, where the moisture content of the air is determined using a hygrometer.
The analysis of the moisture profile over the duration of the measurement allows for the quantification of the amount of moisture removed from the product. Thus, the moisture content of the product in the measurement chamber volume can be reliably determined. With known bulk density, the mass-related moisture content in ppm is obtained.
Unmeasured product and the measured sample are gravimetrically returned to the process.

The DewTector Principle

Advantages

The DewTector‘s® measurement principle is …
↗ simple, as the moisture is extracted from the sample and quantified directly with no need for a costly calibration for each material/recipe (contrary to indirect methods e.g. capacitive, microwave, …).
↗ reliable, as no calibration errors can occur (contrary to indirect methods). The hygrometer reacts exclusively to water and therefore is unaffected by changes in product composition (additives) or the presence of other volatiles that affect e.g. thermogravimetric approaches. 
↗ economic, as it avoids time-consuming and error-prone manual sample taking and analysis.

Technology in Detail

Measurement Accuracy
The measurement accuracy of the DewTector was determined by comparison with Karl Fischer titration (KFT), the most precise laboratory method for moisture measurement. In the test range of 500 … 3500 ppm, accuracy was determined to + 5 … - 15 % vs. KFT.
If higher accuracy is required, simply contact us and we will be happy to discuss the options with you.

Measurement Frequency
Higher moisture content takes longer to be removed for quantification and therefore results in a longer measurement process. Depending on the moisture content, the measurement frequency was determined to:

  Moisture Content

  Measurement Frequency

  ≤ 500 ppm

  10 per hour

  500 … 2500 ppm  

  7 per hour

  2500 … 10000 ppm

  7 … 4 per hour

This allows for quick detection of disturbances as well as tracking long-term trends e.g. due to weather or equipment wear.


Operating Conditions

Bulk Material
In principle, all free-flowing and permeable bulk materials are suitable. Dust in the product is not a problem. We will be happy to test your individual product sample.

Moisture Content
The DewTector can be used for a wide moisture range: from a few hundred to over 10 000 ppm. The product should not be dripping, meaning it should not contain more moisture than it can hold on its particle surfaces and in the inter-particle spaces. Only superficial or easily removable moisture can be captured by the DewTector,

Product Temperature
Maximum: 70 °C (Material resistance)
Minimum: 5 °C (Protection against freezing)

Ambient Temperature
Maximum: 45 °C (Electronics)
Minimum: 5 °C (Protection against freezing)
In case of frost risk: Heating (e.g., heated control cabinet around it)

Dimensions

DTR-A – Automatic Version for Online Measurement
•    Height: approx. 30 cm
•    Width x Depth: approx. 55 x 55 cm

DTR-M – Manual Version for Laboratory Measurement
•    Height: approx. 75 cm
•    Width x Depth: approx. 60 x 60 cm

 

Auxiliary Energies

Power Supply
•    24 VDC, 2.5 A

Pressurized Air
•    Pressure: min. 6 barg max. 12 barg
•    Filter regulator setting: 6 barg
•    Quality: Compressed air according to ISO 8573-1:2010 [7:4:4] The compliance with the maximum content of solid particles and oil is ensured by the integrated filter regulator.

Control and Configuration
The DewTector is connected to the plant's control system via a fieldbus to enable control and transmission of sensor and measurement data.
Configuration is done via a browser using the DewTector Web App provided by the integrated web server.

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